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He Forgot It AlliPad.exe..4 μm, coupled to an Axion-20 photomultiplier. The data and analysis were performed using the Axiomatic framework (Axil Scientific, Inc.) to yield resulting surface area, pore volume, and pore diameter values.
ICP-AES {#Sec22}
——-
The *in situ* elemental analysis was performed using an EOP-SC Advantage (Horiba, J.A.M.M. Equipments) that contained an Nd-YAG laser (λ~ex~ = 266 nm) for plasma generation. A Perkin Elmer Optima 2100 DV ICP-AES (Perkin Elmer, USA) was used for the elemental analysis. The experimental conditions are summarized in Supplementary Table [S1](#MOESM1){ref-type=”media”}. Each experiment was performed in triplicate.
Infrared spectroscopy {#Sec23}
———————
Fourier transform infrared spectroscopy (FTIR, Perkin Elmer, USA) was performed to investigate the chemical changes in the cellulose and lignin degradation. Samples of the degraded lignocellulosic biomass were ground into powder in a small mortar and compressed into disk-shaped specimens. The tests were performed on a Shimadzu FTIR-8400 s spectrometer. The frequency ranging from 600 to 4000 cm^−1^ was used for each experiment. KBr tablets with sample powder were used for FTIR analysis.
Scanning electron microscopy (SEM) {#Sec24}
———————————-
Field emission scanning electron microscopy (FESEM) and energy-dispersive X-ray spectroscopy (EDX) were used to examine the morphological changes in the two biomass samples under different pH conditions. All of the experiments were performed on a Hitachi S-4800 FESEM. SEM samples were prepared by dropping a homogeneous suspension of biomass on a silicon wafer and then allowing them to dry overnight. Accelerating voltages of 10 kV and 20 kV were applied for the FESEM and EDX tests
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